Karl Fischer & Potentiometric Titration Application Library
Determination of chloride ion in concrete | Autotitrator COM-A19
This report introduces an example of the determination of chloride ion in concrete. This measurement method is described in āPotentiometric titration method using chloride ion-selective electrodeā of āJIS A 1154 Method of test for chloride ion content in hardened concreteā. Nitric acid is added to adjust the pH to 3 or less, and extract chloride ion with boiling. Cool to room temperature, filtrate to separate undissolved component and collect filtrated solution as sample. Chloride ion is determined by precipitation titration using a silver nitrate standard solution.
Determination of chloride ion in cement | Autotitrator COM-A19
This report introduces an example of the determination of chloride ion in cement. This measurement method is described in āMethod for measuring chlorideā of āJapanese industrial standard JIS R 5202 Method for chemical analysis of cementsā. The sample is dissolved in nitric acid, a chloride ion standard solution and a hydrogen peroxide solution are added, and the sample is heat-treated, and then the measurement is performed by precipitation titration using a silver nitrate standard solution. The measurements are made by potentiometric titration using a chloride ion-selective electrode as the electrode for end point detection.
